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A NEW RP-HPLC METHOD DEVELOPMENT AND VALIDATION FOR THE SIMULTANEOUS ESTIMATION OF EMTRICITABINE AND TENOFOVIR IN PHARMACEUTICAL DOSAGE FORMS

📘 Volume 11 📄 Issue 4 📅 April 2026

👤 Authors

G. N. Rajeswari, G. U. Jayanthi, G. B. A. Sindhu, M. Poojateswari, M. Bhanu Prakash, M. J. R. Sanjana, V. Bhaskara Raju, K. S. Sumanth 1
1. Department of Pharmaceutical Analysis, Pharmaceutical Analysis, Sri Vasavi Institute of Pharmaceutical Sciences, Pedatadepalli, Tadepalligudem, Andhra Pradesh, India

📄 Abstract

A new, simple and rapid RP-HPLC method was developed and validated for the estimation of EMTRICITABINE and TENOFOVIR in pharmaceutical dosage forms. The chromatographic separation was achieved on SHISEIDO C18 column (250 x 4.6 mm i.d, 5µ) using Methanol: 20nM phosphate buffeer (pH 5.0±0.05) in the ratio of 35:65v/v, with a flow rate of 1 ml/min and detection at 271 nm. The retention times for EMT and TEN were found to be 2.80 and 4.81 min respectively. Linearity was established in the range of 10-60µg/ml for both EMT and TEN respectively. The method was precise with %RSD < 2 for both intraday and interday precision. The accuracy of the method was performed over three levels of concentration and the recovery was in the range of 98-102%.

🏷️ Keywords

Emtricitabine Tenofovir RP-HPLC Method development Validation

📚 How to Cite:

G. N. Rajeswari, G. U. Jayanthi, G. B. A. Sindhu, M. Poojateswari, M. Bhanu Prakash, M. J. R. Sanjana, V. Bhaskara Raju, K. S. Sumanth , A NEW RP-HPLC METHOD DEVELOPMENT AND VALIDATION FOR THE SIMULTANEOUS ESTIMATION OF EMTRICITABINE AND TENOFOVIR IN PHARMACEUTICAL DOSAGE FORMS , Volume 11 , Issue 4, April 2026, EPRA International Journal of Research & Development (IJRD) ,

🔗 PDF URL

https://cdn.eprapublishing.org/article/202604-02-027349.pdf

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